Effect of sintering temperature on carbonated hydroxyapatite derived from common cockle shells (Cerastodermaedule): Composition and crystal characteristics

Wati, Rosita and Yusuf, Yusril (2019) Effect of sintering temperature on carbonated hydroxyapatite derived from common cockle shells (Cerastodermaedule): Composition and crystal characteristics. Key Engineering Materials, 818 KE. 37 - 43. ISSN 10139826

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Abstract

Incorporation carbonate ion to hydroxyapatite (HAp) structure, known as carbonated hydroxyapatite (CHAp) is reported to reduce crystallinity, increase the solubility rate, and increase bioactivity. Sintered CHAp material is interesting because it may have a better biological response.CHAp derived from common cockle (Cerastoderma edule) shell have produced by precipitation method. This study aimed to investigate the effect of sintering temperature to compositon and crystal characteristics of CHAp. CHAp powder was sintered at 400, 600, and 800<sup>o</sup> C in air atmosphere.CHApas-preparedand sintered samples were analyzed using Energy Dispersive Spectrometry (EDS), Fourier Transform Infrared (FT-IR), and X-ray Diffractometer (XRD).EDS analysis showed that the Ca/P ratio of powder CHAp was around 1.67-1.94 (greater than the Ca/P ratioof HAp). For increasing of sintering temperature, carbonate and water content decreased, crystallinity and crystallite size increased. © 2019 Trans Tech Publications, Switzerland.

Item Type: Article
Additional Information: Cited by: 11
Uncontrolled Keywords: Carbonation; Crystallinity; Crystallite size; Hydroxyapatite; Mechanics; Shellfish; Carbonated hydroxyapatites; Cerastoderma edule; Common cockle shells; Precipitation methods; Sintering temperatures; Sintering
Subjects: Q Science > QC Physics
Divisions: Faculty of Mathematics and Natural Sciences > Physics Department
Depositing User: Sri JUNANDI
Date Deposited: 01 Jul 2026 00:46
Last Modified: 01 Jul 2026 00:46
URI: https://ir.lib.ugm.ac.id/id/eprint/25438

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