Fast and selective colorimetric detection of Fe<SUP>3+</SUP> based on gold nanoparticles capped with ortho-hydroxybenzoic acid

Andreani, Agustina Sus and Kunarti, Eko Sri and Hashimoto, Takeshi and Hayashita, Takashi and Santosa, Sri Juari (2021) Fast and selective colorimetric detection of Fe<SUP>3+</SUP> based on gold nanoparticles capped with ortho-hydroxybenzoic acid. JOURNAL OF ENVIRONMENTAL CHEMICAL ENGINEERING, 9 (5). ISSN 2213-2929

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Abstract

A fast and selective colorimetric sensor for detecting Fe3+ was developed using gold nanoparticles capped with ortho-hydroxybenzoic acid (o-HBA AuNPs). This sensor was characterized using UV-Vis spectroscopy, FTIR spectroscopy, XRD, and TEM. The absorbance of surface plasmon resonance (SPR) at 534 nm increased after the addition of Fe3+. It was confirmed by FTIR, XRD, and TEM data indicating that Fe3+ acted as a bridge among the capping agents of AuNPs. The bridges blocked AuNPs from aggregation and caused an increase in the uniformity distribution of o-HBA AuNPs. Under the optimized condition, this sensor had a good calibration curve linearity at 534 nm. The value of R-2 obtained was 0.9994 with LoD of 9.19 mu M and LoQ of 30.57 mu M. This sensor exhibited good precision and accuracy for Fe3+ detection in rice field, river, and sea waters and has been successfully used to detect Fe3+ in the real water samples collected from various locations of Code River, Yogyakarta, Indonesia.

Item Type: Article
Uncontrolled Keywords: Fe3+; O-HBA AuNPs; Colorimetric detection; Ortho-hydroxybenzoic acid
Subjects: Q Science > QD Chemistry
Divisions: Faculty of Mathematics and Natural Sciences > Chemistry Department
Depositing User: Sri JUNANDI
Date Deposited: 18 Oct 2024 01:07
Last Modified: 18 Oct 2024 01:07
URI: https://ir.lib.ugm.ac.id/id/eprint/9273

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