Application of Fourier Transform Near-Infrared (FT-NIR) spectroscopy for detection of adulteration in palm sugar

Rismiwandira, K. and Roosmayanti, F. and Pahlawan, M. F. R. and Masithoh, R. E. (2021) Application of Fourier Transform Near-Infrared (FT-NIR) spectroscopy for detection of adulteration in palm sugar. IOP Conference Series: Earth and Environmental Science, 653 (1). ISSN 17551307

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Abstract

The aim of this research was to detect adulteration in palm sugar by coconut sugar using FT-NIR spectroscopy with two chemometric methods namely partial least squares regression (PLSR) and principal component analysis (PCA). The absorbance spectra were taken using the FT-NIRFlex-500 Solid. Several spectral pre-processing methods used were the 1st Savitzky-Golay Derivative, Normalization, Standard Normal Variate (SNV), Multiplicative Scatter Correction (MSC), and Baseline. Coconut sugar as adulterant with various concentration ranging from 0 to 100 were added to the palm sugar. A total of 77 spectra of pure and adulterated palm sugar samples were divided into two groups in which 51 samples used for developing calibration model and 26 samples used for developing prediction model. The spectral obtained were pre-processed and analyzed using The Unscrambler X version 10.4. The best transformation of PLSR was MSC with coefficient of determination (Rc2) of 0.93 and the root mean square error (RMSE) of 0.07 for calibration. By using prediction data sets, the model resulted in coefficient of determination of prediction (Rp2) of 0.91 and a root mean square error of prediction (RMSEP) of 0.09. Based on this result, FT-NIR spectroscopy combined with chemometrics is a promising method in food authentication.

Item Type: Article
Additional Information: Library Dosen
Uncontrolled Keywords: Agriculture; Forecasting; Infrared devices; Mean square error; Near infrared spectroscopy; Palmprint recognition; Predictive analytics; Regional planning; Coefficient of determination; Fourier transform near infrared spectroscopy; Multiplicative scatter correction; Partial least squares regressions (PLSR); Pre-processing method; Root mean square errors; Root-mean-square error of predictions; Standard normal variates; Least squares approximations
Subjects: S Agriculture > S Agriculture (General)
T Technology > TJ Mechanical engineering and machinery > Agricultural machinery. Farm machinery
Divisions: Faculty of Agricultural Technology > Agricultural and Biosystems Engineering
Depositing User: Sri JUNANDI
Date Deposited: 22 Oct 2024 06:09
Last Modified: 22 Oct 2024 06:09
URI: https://ir.lib.ugm.ac.id/id/eprint/5463

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